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FA | RX(1); FLST(1); RX(1) |
Reaction (1 of 1)
Reaction ID | 1767834 |
Reactant BRN | 136380; 1098295 |
Reactant | 5-allyl-benzo[1,3]dioxole; tetrachloromethane |
Product BRN | 4524942; 4448026 |
Product | 2-benzo[1,3]dioxol-5-ylmethyl-4,4,4-trichloro-butyric acid ethyl ester; 1,2-methylenedioxy-4-(2,4,4,4-tetrachlorobutyl)benzene |
No. of Reaction Details | 1 |
Reaction Details (1 of 1)
Reaction Classification | Preparation |
Yield | 35 percent (BRN=4448026); 29 percent (BRN=4524942) |
Reagent | Pd(OAc)2, PPh3, K2CO3, CO |
Solvent | ethanol |
Time | 48 hour(s) |
Temperature | 80 |
Pressure | 30400.004 |
Citation Pointer | 5543032; Journal; Tsuji, Jiro; Sato, Koji; Nagashima, Hideo; TELEAY; Tetrahedron Lett.; EN; 23; 8; 1982; 893-896; |
Reference (1 of 1)
Citation Number | 5543032 |
Document Type | Journal |
Authors | Tsuji, Jiro; Sato, Koji; Nagashima, Hideo |
CODEN | TELEAY |
Journal Title | Tetrahedron Lett. |
Language Code | EN |
(Series) Volume | 23 |
Number | 8 |
Publication Year | 1982 |
Page | 893-896 |